Example 12.2: A slurry is filtered in a plate and frame press, containing 12 frames, each having a square cross section with 0.3 m in length and width, and 25 mm thick. During the first 200 seconds, the filtration pressure is slowly raised to a final value of 500 kilo Newton per m2, and during this period the rate of filtration is kept constant. After the initial period, filtration is carried out at constant pressure, and the cake is completely formed in a further 900 seconds. The cakes are then washed at 375 kilo Newton per m2 for 600 seconds using thorough washing. What is the volume of the filtrate collected per cycle and how much wash water is used? Given L over v as 0.35 cm, and r μ v as 7.13 time10-4 kilo Newton second m2 per cm6.
Solution:
Cross-sectional area of bed, A, is equal to 2 n LF WF or 2.16 m2. And total pressure drop is 500 minus 101.3 or 398.7 kilo Newton per m2. The constant B1r for constant rate operation is A L over nu or 7.56 time 103 cm3.
The constants B2r is equal to minus delta p2 over r mu nu. Its value is found to be 2.609 time 106 cm6 per second. And volume of filtrate collected at the end of constant filtration rate period is 1.937 time 104 cm3.
In the second step, filtration is conducted at constant pressure. Properties of cake and cloth and filtrate do not change.The values of B1p for constant pressure operation is 2 B1r and is equal to 1.512 time 104 cm3. The values of B2p for constant pressure operation is 2 B2r and is equal to 5.218 time 106 cm6 per second. This volume contains filtrate from both kinds of operations. Volume and t relationship written for two time t1 and t can be used to write equation such as (V2 minus V12) plus B1 time (V minus V1) equals B2 time (t minus t1).The above equation is quadratic in V and can be rewritten as V2 plus B1V minus C is equal to zero. The constant C is equal to V12 plus B1V plus B2 time (t minus t1). In this equation t1 represents the time constant filtration rate operation during which volume of filtrate cllected is V1. After a total time, t2, of 1100 s, V2 can be calculated as 6.607 time 104 cm3.
Final rate of filtration is B2p over (2V2 plus B1p). Its value is found to be 35.43 cm3 per sec. Cake washing is done at a pressure less than the filtration pressure. Cake is washed at a rate that is proportional to the final filtration rate. If washing pressure is P3, then washing rate can be calculated as (375 minus 101.03) over (500 minus 101.03) time 35.43 or 24.32 cm3 per sec. If cake is washed for a period of t3, water requirement can be estimated as 24.32 time 600 or 1.459 time 104 cm3.